3-甲基-5-苯基-4-异噁唑甲醛合成路线 （共 6 条）
反应条件
hydrogenchloride; diisobutylaluminium hydride in toluene
参考文献
Green, Jeremy; Bemis, Guy; Grillot, Anne-Laure; Ledeboer, Mark; Salituro, Francesco G.; Harrington, Edmund; Gao, Huai; Baker, Christopher; Cao, Jingrong; Hale, Michael
Patent: US2003/149051 A1, 2003 ;
反应条件
sodium dichromate; sulfuric acid in dimethyl sulfoxide 1. 50 deg C 2. 1h 70 deg C;
参考文献
Heck, Reinhard; Ofenloch, Roland; Wolf, Roland
Synthesis, 1990 , # 1 p. 62 - 64
反应条件
1: 1. Cl-CO2Et, Et3N 2. NaBH4 / 1. THF, -10 deg C, 30 min 2. a. H2O, 5-10 deg C b. 3h, room temperature 2: 70 percent / Na2Cr2O7*2H2O, H2SO4 / dimethylsulfoxide / 1. 50 deg C 2. 1h 70 deg C View Scheme
参考文献
Synthesis, , # 1 p. 62 - 64
反应条件
n-butyllithium 1.) -78 deg C, 5 h, 2.) 25 deg C, 1 h;
参考文献
Alberola, Angel; Calvo, Luis; Rodriguez, M. Teresa Rodriguez; Sanudo, M. Carmen
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 2 p. 537 - 542
反应条件
oxygen 1. chloroform, 0 degC, 1d; 2. chloroform, r.t., 3d; Yield given. Multistep reaction;
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 1505 - 1507
反应条件
in chloroform-d1
acetonitrile was added in 6 portions during two weeks;
参考文献
De Sarlo, Francesco; Guarna, Antonio; Brandi, Alberto
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1505 - 1507
