2-甲氧基-2-甲基丙胺合成路线 （共 13 条）
反应条件
1: With lithium aluminium tetrahydride in diethyl ether T=0°C; 7 h; Heating / reflux; 2: With sodium hydroxide; water in diethyl ether T=0 - 20°C; 14 h;
参考文献
WO2006/97808 A1, ;
Page/Page column 66-67 ;
WO 2006/097808 A1
反应条件
hydrogenchloride; sodium hydroxide; hydrazine in N-methyl-acetamide; methanol; chloroform; water
参考文献
Institute of Nuclear Energy Research
Patent: US5210270 A1, 1993 ;
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 72, p. 2657,2659
反应条件
sodium methylate in methanol
反应条件
ethanol; nickel T=18°C; P=80905.8 Torr; Hydrogenation;
参考文献
Zhurnal Obshchei Khimii, , vol. 22, p. 2121,2124;engl.Ausg.S.2175,2178
反应条件
1: water; methanol; ammonia 2: lithium alanate; diethyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 72, p. 2657,2659
反应条件
hydrazine in methanol Product distribution / selectivity;
参考文献
US2008/102028 A1, ;
Page/Page column 9; -11 ;
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran 3 h; Product distribution / selectivity;
参考文献
DRAXIS Specialty Pharmaceuticals Inc.
Patent: US2008/102028 A1, 2008 ;
Location in patent: Page/Page column 9; 10-11 ;
反应条件
(i) BF3, (ii) KOH; Multistep reaction;
参考文献
Chemische Berichte, , vol. 97, p. 510 - 519
参考文献
Hao, Guiyang; Zang, Jianying; Liu, Boli
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 1 p. 13 - 18
