5,6,7,8-四氢-4-羟基-2-萘羧酸甲酯合成路线 (共 4 条)
反应条件
quinoline; sodium hydroxide; water; copper 1.) THF, 25-60 deg C, 12-25 h; 2.) 210-260 deg C, 1-7 h; Yield given. Multistep reaction;
参考文献
Boger, Dale B.; Mullican, Michael D.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4033 - 4044
反应条件
in 1,3,5-trimethyl-benzene
T=180°C; 40 h;
参考文献
Boger, Dale L.; Mullican, Michael D.
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 4939 - 4942
Title/Abstract Full Text View citing articles Show Details
Boger, Dale B.; Mullican, Michael D.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4033 - 4044
反应条件
1: 84 percent / lithium diisopropylamide / tetrahydrofuran / 2.75 h / -30 - 25 °C
2: 83 percent / 1,3,5-trimethyl-benzene / 40 h / 180 °C
View Scheme
参考文献
Boger, Dale B.; Mullican, Michael D.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4033 - 4044
反应条件
hydrogenchloride; sulfuric acid
参考文献
Sergiewskaja; Popowa
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 153,155; engl. Ausg. S. 155