暂无反应条件数据

trichlorophosphate T=120°C;

copper; potassium carbonate in N,N-dimethyl-formamide T=150°C; 2 h;

copper in 3-methyl-1-butanol 21 h; Heating;

copper diacetate; sodium acetate in water Reflux;

3-methyl-1-butanol; copper; potassium carbonate

暂无反应条件数据

1: 83 percent / H2O; ethanol / 1.25 h / 100 °C 2: 96 percent / H2O / 2 h / 35 - 40 °C 3: 78 percent / 25percent NaOH / H2O / 2 h / Heating 4: 1.) 25percent aq. NaOH / 1.) DMF, room temp., 30 min; 2.) room temp., 3 h, 50 - 55 deg C, 30 min 5: 82 percent / sodium methoxide / methanol / 1.5 h / Heating 6: potassium carbonate / acetone / 24 h / Heating 7: 74 percent / potassium t-butoxide / tetrahydrofuran / 18 h 8: 80 percent / potassium carbonate / acetone / 48 h / Heating 9: 10percent aqueous NaOH / aq. ethanol / 1.5 h / Heating View Scheme

1: 83 percent / H2O; ethanol / 1.25 h / 100 °C 2: 96 percent / H2O / 2 h / 35 - 40 °C 3: 78 percent / 25percent NaOH / H2O / 2 h / Heating 4: 1.) 25percent aq. NaOH / 1.) DMF, room temp., 30 min; 2.) room temp., 3 h, 50 - 55 deg C, 30 min 5: 82 percent / sodium methoxide / methanol / 1.5 h / Heating 6: potassium carbonate / acetone / 24 h / Heating 7: 74 percent / potassium t-butoxide / tetrahydrofuran / 18 h 8: 80 percent / potassium carbonate / acetone / 48 h / Heating 9: 72 percent / anhydrous ammonia, lithium / hydrated ferric nitrate / tetrahydrofuran / 16 h View Scheme

formaldehyd in ethanol; sodium hydrogencarbonate