perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile T=83°C; 0.416667 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

1: magnesium / diethyl ether 2: S2O8(2-), HClO4 / Cu(ClO4)2 / acetonitrile; H2O / 0.42 h / 83 °C View Scheme

perchloric acid; hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile T=83°C; 0.416667 h; other reaction condition; MechanismProduct distribution;