3-氨基-1-甲基吡唑-5-羧酸甲酯合成路线 （共 10 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethanol; ethyl acetate P=2585.81 Torr; 2.5 h;
参考文献
WO2011/140488 A1, ;
Page/Page column 167; 168 ;
WO 2011/140488 A1
反应条件
hydrogen; palladium 10 on activated carbon in ethanol P=1551.49 Torr; 16 h;
参考文献
WO2004/98589 A1, ;
Page 166 ;
WO 2004/098589 A1
反应条件
potassium hydroxide; hydroxylamine hydrochloride in ethanol; water Heating;
参考文献
Journal of Organic Chemistry, , vol. 49, # 7 p. 1224 - 1227
反应条件
hydrogen; palladium on activated charcoal P=2660 Torr; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: 68 percent / aq. H2SO4 / 18 h / Heating 2: SOCl2 / 0.5 h / Heating 3: NaN3 / acetone; H2O / 0.02 h 4: toluene / 0.5 h / Heating 5: 100 percent / H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: SOCl2 / 0.5 h / Heating 2: NaN3 / acetone; H2O / 0.02 h 3: toluene / 0.5 h / Heating 4: 100 percent / H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: NaN3 / acetone; H2O / 0.02 h 2: toluene / 0.5 h / Heating 3: 100 percent / H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
1: toluene / 0.5 h / Heating 2: 100 percent / H2 / 5percent Pd/C / 0.5 h / 2660 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 2 p. 428 - 431
反应条件
sodium hydroxide; 3-chloro-benzenecarboperoxoic acid in chloroform
参考文献
Pharmacia S.p.A.
Patent: US5753629 A1, 1998 ;
反应条件
in N,N-dimethyl-formamide 2 h;
参考文献
Ding, Lu; Grehn, Leif; Ragnarsson, Ulf
Acta Chemica Scandinavica, 1990 , vol. 44, # 1 p. 75 - 81
