5,10-四甲基茚并[2,1-a]茚合成路线 （共 3 条）
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C; 3 h;
2: With hydrogenchloride in tetrahydrofuran; hexane; water
参考文献
SAMSUNG DISPLAY CO., LTD.; Kim, Soo-Yon; Hwang, Seok-Hwan; Kim, Young-Kook; Jung, Hye-Jin; Lim, Jin-O; Han, Sang-Hyun; Jeong, Eun-Jae; Park, Jun-Ha; Lee, Eun-Young; Lee, Bo-Ra; Lee, Jong-Hyuk
Patent: US2014/27721 A1, 2014 ;
Location in patent: Paragraph 0127; 0131 ;
反应条件
palladium on activated charcoal
T=340 - 350°C;
参考文献
Hancock,J.E.H.; Pavia,D.L.
Journal of Organic Chemistry, 1961 , vol. 26, p. 4350 - 4352
反应条件
in tetrahydrofuran
Yield given;
参考文献
Hellwinkel, Dieter; Hasselbach, Hans-Joachim; Laemmerzahl, Frank
Angewandte Chemie, 1984 , vol. 96, # 9 p. 713 - 714
