palladium 10 on activated carbon; hydrogen in methanol P=10343.2 Torr; 12 h; Inert atmosphere;

1: methanol; potassium carbonate / 2 h / 20 °C / Inert atmosphere 2: ethanol / 4 h / 100 °C / Inert atmosphere 3: palladium 10 on activated carbon; hydrogen / methanol / 12 h / 10343.2 Torr / Inert atmosphere View Scheme

1: ethanol / 4 h / 100 °C / Inert atmosphere 2: palladium 10 on activated carbon; hydrogen / methanol / 12 h / 10343.2 Torr / Inert atmosphere View Scheme

T=600°C; P=0.001 - 0.01 Torr; 0.5 h;

T=600°C; 1.5 h;

1: 90 percent / triethyl orthoformate 2: 0.5 h / 600 °C / 0 - 0.01 Torr View Scheme