(2-溴-3-苯基丙基)苯合成路线 (共 5 条)
反应条件
titanium (IV) bromide in dichloromethane
T=-78°C; 2.5 h; Inert atmosphere;
参考文献
Lepore, Salvatore D.; Mondal, Deboprosad; Song, Ye Li; Bhunia, Anjan K.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 39 p. 7511 - 7514
反应条件
titanium (IV) bromide in dichloromethane
T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Lepore, Salvatore D.; Mondal, Deboprosad; Song, Ye Li; Bhunia, Anjan K.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 39 p. 7511 - 7514
反应条件
trichloromonobromomethane; Fonderma; 4-(N,N-dimethlyamino)pyridine
T=105°C; 1 h;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
hydrogen bromide
T=100 - 120°C;
参考文献
Edgerton et al.
Journal of the American Pharmaceutical Association (1912-1977), 1959 , vol. 48, p. 320,323
反应条件
trichloromonobromomethane; Fonderma; 4-(N,N-dimethlyamino)pyridine
2.) reflux; Yield given. Multistep reaction;
参考文献
Barton, Derek H.R.; Crich, David; Motherwell, William B.
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 4979 - 4982