乙基4-(4-碘苯甲酰基)苯甲酸酯合成路线 (共 1 条)
反应条件
1: 4-iodobenzoic acid ethyl ester; iso-propylmagnesium bromide in tetrahydrofuran T=0°C; 0.333333 h; Inert atmosphere; 2: bis(1,3-benzothiazol-2-yl)methanone in tetrahydrofuran T=0°C; 1 h; Inert atmosphere; 3: With (NH4)2SO4 in tetrahydrofuran; water Inert atmosphere; regioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 29 p. 5659 - 5665