1,5-二甲基-6,8-二氧杂双环[3.2.1]辛烷-7-酮合成路线 （共 5 条）
反应条件
in diethyl ether
7 h; Ambient temperature;
参考文献
Utaka, Masanori; Makino, Hiroshi; Oota, Yukito; Tsuboi, Sadao; Takeda, Akira
Tetrahedron Letters, 1983 , vol. 24, # 25 p. 2567 - 2570
反应条件
2: LiAlH4
3: 1.) NaH
4: Heating
View Scheme
参考文献
Utaka, Masanori; Makino, Hiroshi; Oota, Yukito; Tsuboi, Sadao; Takeda, Akira
Tetrahedron Letters, 1983 , vol. 24, # 25 p. 2567 - 2570
反应条件
sodium tetrahydroborate; aluminium trichloride in tetrahydrofuran
Reduction; 2.5 h; Heating;
参考文献
Jun, Jong-Gab; Lee, In-Suk
Synthetic Communications, 2000 , vol. 30, # 7 p. 1159 - 1165
反应条件
sodium tetrahydroborate
Title compound not separated from byproducts;
参考文献
Utaka, Masanori; Tsuboi, Sadao; Makino, Hiroshi; Oota, Yukito; Takeda, Akira
Heterocycles, 1984 , vol. 21, # 2 p. 603
反应条件
in diethyl ether
7 h; Ambient temperature;
参考文献
Utaka, Masanori; Makino, Hiroshi; Oota, Yukito; Tsuboi, Sadao; Takeda, Akira
Tetrahedron Letters, 1983 , vol. 24, # 25 p. 2567 - 2570
