(2E)-1-(2-羟基苯基)-3-苯基-2-丙烯-1-酮合成路线 (共 83 条)
反应条件
trimethylsilylazide 56 h; Ambient temperature;
参考文献
Acta Chimica Hungarica, , vol. 114, # 1 p. 47 - 56
反应条件
1: 96 percent / pyridine / 12 h / 20 °C 2: 620 mg / benzene / 15 h / Irradiation View Scheme
参考文献
Norikane, Yasuo; Itoh, Hiroki; Arai, Tatsuo
Journal of Physical Chemistry A, 2002 , vol. 106, # 11 p. 2766 - 2776
反应条件
dihydrogen peroxide; diethylamine in 1,4-dioxane; water T=5°C; Algar-Flynn-Oyamada reaction; 40 h;
参考文献
Loeser, Reik; Chlupacova, Marta; Marecek, Ales; Opletalova, Veronika; Guetschow, Michael
Helvetica Chimica Acta, 2004 , vol. 87, # 10 p. 2597 - 2601
反应条件
potassium hydroxide; cyclohexane-1,1-diyl bis-hydro peroxide in 1,4-dioxane T=20°C; 3.5 h;
参考文献
Jakka, Kavitha; Liu, Jinyun; Zhao, Cong-Gui
Tetrahedron Letters, 2007 , vol. 48, # 8 p. 1395 - 1398
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone 1.) 0 deg C to room temperature, 14 h, 2.) room temperature, 24 h, 3.) 0 deg C to room temperature, 43.5 h;
参考文献
Burke, Anthony J.; O'Sullivan, W. Ivo
Tetrahedron, 1997 , vol. 53, # 25 p. 8491 - 8500
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide in 1,4-dioxane 3.5 h; Ambient temperatureother chalcones; Mechanism;
参考文献
Saxena, Shabnam; Makrandi, J. K.; Grover, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 473 - 477
反应条件
in benzene Irradiationsensitized (rose bengal) photooxygenation; Mechanism;
参考文献
Chawla, H. M.; Chakrabarty, Kakoli; Prakash, Anil; Chibber, S. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 507 - 508
反应条件
Irradiationsensitized (rose bengal) photooxygenation; other solvent (ethanol); Mechanism;
参考文献
Chawla, H. M.; Chakrabarty, Kakoli; Prakash, Anil; Chibber, S. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 507 - 508
反应条件
potassium hydroxide; ethanol
0.0333333 h; Microwave irradiation;
参考文献
Krohn, Karsten; Ahmed, Ishtiaq; John, Markus
Synthesis, 2009 , # 5 p. 779 - 786
反应条件
1: 45 percent / aq. KOH / ethanol / 120 h / 0 - 5 °C
2: 10 percent aq. NaOH / ethanol / 20 °C
View Scheme
参考文献
Mphahlele, Malose J.; Fernandes, Manuel A.
South African Journal of Chemistry, 2002 , vol. 55, p. 97 - 110