反应条件
1: 2-bromo-3,4-dimethyl-2-cyclopenten-1-one ethylene ketal With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-78 - -30°C; 2 h;
3: With hydrogenchloride in tetrahydrofuran; hexane; water