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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
西拉普利
合成路线
（共 14 条）
106860-19-9
→
反应条件
88768-40-5
西拉普利
反应条件
hydrogenchloride in dichloromethane 16 h; Ambient temperature;
参考文献
Attwood, Michael R.; Hassall, Cedric H.; Kroehn, Antonin; Lawton, Geoffrey; Redshaw, Sally
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1011 - 1020
29678-81-7
(R)-2-羟基-4-苯基丁酸
→
反应条件
88768-40-5
西拉普利
反应条件
1: 97 percent / cc. H2SO4 / 2 h / Heating 2: 85 percent / CH2Cl2; pyridine / 2 h / 10 °C 3: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 4: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
88767-16-2
→
反应条件
88768-40-5
西拉普利
反应条件
1: NaHCO3 / toluene; H2O / 17 h / Ambient temperature 2: H2 / 5percent Pd-C / dimethylformamide / 18 h 3: SOCl2 / CH2Cl2 / 4 h / Ambient temperature 4: 90 percent / 1M borane in THF / tetrahydrofuran / 3 h / Ambient temperature 5: hydrazine hydrate / ethanol / 1 h / Ambient temperature 6: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 7: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
106860-13-3
→
反应条件
88768-40-5
西拉普利
反应条件
1: H2 / 5percent Pd-C / dimethylformamide / 18 h 2: SOCl2 / CH2Cl2 / 4 h / Ambient temperature 3: 90 percent / 1M borane in THF / tetrahydrofuran / 3 h / Ambient temperature 4: hydrazine hydrate / ethanol / 1 h / Ambient temperature 5: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 6: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
72064-51-8
(S)-四氢-1,3(2H)-哒嗪二羧酸 3-叔丁酯 1-(苯甲基)酯
→
反应条件
88768-40-5
西拉普利
反应条件
1: NaHCO3 / toluene; H2O / 17 h / Ambient temperature 2: H2 / 5percent Pd-C / dimethylformamide / 18 h 3: SOCl2 / CH2Cl2 / 4 h / Ambient temperature 4: 90 percent / 1M borane in THF / tetrahydrofuran / 3 h / Ambient temperature 5: hydrazine hydrate / ethanol / 1 h / Ambient temperature 6: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 7: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
88784-33-2
(S)-2-(1,3-二氧代-1,3-二氢异吲哚-2-基)戊二酸-5-苄酯
→
反应条件
88768-40-5
西拉普利
反应条件
1: SOCl2 / toluene 2: NaHCO3 / toluene; H2O / 17 h / Ambient temperature 3: H2 / 5percent Pd-C / dimethylformamide / 18 h 4: SOCl2 / CH2Cl2 / 4 h / Ambient temperature 5: 90 percent / 1M borane in THF / tetrahydrofuran / 3 h / Ambient temperature 6: hydrazine hydrate / ethanol / 1 h / Ambient temperature 7: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 8: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
88767-18-4
→
反应条件
88768-40-5
西拉普利
反应条件
1: SOCl2 / CH2Cl2 / 4 h / Ambient temperature 2: 90 percent / 1M borane in THF / tetrahydrofuran / 3 h / Ambient temperature 3: hydrazine hydrate / ethanol / 1 h / Ambient temperature 4: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 5: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
106927-97-3
(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-10-氧代-6H-哒嗪并[1,2-A][1,2]二氮杂卓-1-羧酸叔丁酯
→
反应条件
88768-40-5
西拉普利
反应条件
1: hydrazine hydrate / ethanol / 1 h / Ambient temperature 2: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 3: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
106928-72-7
(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-6,10-二氧代-6H-哒嗪并[1,2-a][1,2]二氮杂卓-1-羧酸叔丁酯
→
反应条件
88768-40-5
西拉普利
反应条件
1: 90 percent / 1M borane in THF / tetrahydrofuran / 3 h / Ambient temperature 2: hydrazine hydrate / ethanol / 1 h / Ambient temperature 3: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 4: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
90315-82-5
(R)-2-羟基-4-苯基丁酸乙酯
→
反应条件
88768-40-5
西拉普利
反应条件
1: 85 percent / CH2Cl2; pyridine / 2 h / 10 °C 2: 10percent aq. Na2CO3 / CH2Cl2 / 5 h / Ambient temperature 3: 91 percent / HCl / CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1011 - 1020
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