5,11-二氢-6H-吡啶并[2,3-B][1,4]苯并二氮杂-6-酮合成路线 （共 23 条）
反应条件
T=205°C; 0.0833333 h;
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 17 p. 4300 - 4315
反应条件
palladium on activated charcoal in pyridine 24 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, # 5 p. 1329 - 1334
反应条件
palladium on activated charcoal in pyridine 2 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, # 5 p. 1329 - 1334
反应条件
potassium tert-butylate in 1,4-dioxane T=25 - 100°C; 2.75 h; microwave irradiation;
参考文献
Tetrahedron, , vol. 59, # 6 p. 781 - 787
反应条件
1: 86 percent / aq. HCl; SnCl2 / 0.25 h / 100 °C 2: 80 percent / 0.08 h / 205 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 17 p. 4300 - 4315
反应条件
1: oxalyl chloride; DMF / tetrahydrofuran / 1 h / Heating 2: 5.55 g / pyridine / tetrahydrofuran / 2 h / 20 °C 3: 86 percent / aq. HCl; SnCl2 / 0.25 h / 100 °C 4: 80 percent / 0.08 h / 205 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 17 p. 4300 - 4315
反应条件
1: 5.55 g / pyridine / tetrahydrofuran / 2 h / 20 °C 2: 86 percent / aq. HCl; SnCl2 / 0.25 h / 100 °C 3: 80 percent / 0.08 h / 205 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 17 p. 4300 - 4315
反应条件
in various solvent(s) T=115°C; 24 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 35, # 3 p. 675 - 686
反应条件
5 percent palladium-carbon in pyridine 17 h; Heating;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 53, # 8 p. 1820 - 1844
反应条件
1: acetonitrile / 3 h / Heating 2: 28 percent / acetic acid / 11 h / Heating 3: 5percentPd on active carbon / pyridine / 17 h / Heating View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 53, # 8 p. 1820 - 1844
