5,5-二甲基-2-苯氧基-1,3,2-二氧杂磷杂环己烷 2-氧化物合成路线 （共 10 条）
反应条件
1: CCl4 / 0 - 10 °C 2: solvolysis View Scheme
参考文献
Blackburn, G. Michael; Ingleson, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1150 - 1153
参考文献
McConnell; Coover
Journal of Organic Chemistry, 1959 , vol. 24, p. 630,634
反应条件
dinitrogen tetraoxide in dichloromethane
T=-60°C;
参考文献
Arshinova, R.P.; Kadyrov, R.A.; Klochkov, V.V.; Aganov, A.V.; Shakirov, I.Kh.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2301 - 2305
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2512 - 2517
参考文献
McConnell; Coover
Journal of Organic Chemistry, 1959 , vol. 24, p. 630,634
反应条件
2: N2O4 / CH2Cl2 / -60 °C
View Scheme
参考文献
Arshinova, R.P.; Kadyrov, R.A.; Klochkov, V.V.; Aganov, A.V.; Shakirov, I.Kh.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2301 - 2305
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2512 - 2517
反应条件
2: N2O4 / CH2Cl2 / -60 °C
View Scheme
参考文献
Arshinova, R.P.; Kadyrov, R.A.; Klochkov, V.V.; Aganov, A.V.; Shakirov, I.Kh.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2301 - 2305
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2512 - 2517
反应条件
1: 90 percent / triethylamine / toluene / 0.5 h / 0 °C
2: ozone / toluene; CH2Cl2 / -78 °C
3: toluene; CH2Cl2 / -50 °C
View Scheme
参考文献
Khatib, F. el; Caminade, A. M.; Koenig, M.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 20, p. 55 - 66
反应条件
1: 90 percent / triethylamine / toluene / 0.5 h / 0 °C
2: ozone / toluene; CH2Cl2 / -78 °C
3: toluene; CH2Cl2 / -50 °C
View Scheme
参考文献
Khatib, F. el; Caminade, A. M.; Koenig, M.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 20, p. 55 - 66
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide in chlorobenzene
T=30°C; KineticsMechanism;
参考文献
Rueger, C.; Koenig, T.; Schwetlick, K.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 4 p. 622 - 632
反应条件
in dichloromethane; toluene
T=-50°C;
参考文献
Khatib, F. el; Caminade, A. M.; Koenig, M.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 20, p. 55 - 66
