2-(三甲基硅)苯基三氟甲烷磺酸盐合成路线 （共 525 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; cesium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran; acetonitrile T=60°C; Elimination; Cyclization; 24 h; Title compound not separated from byproducts;
参考文献
Yoshikawa, Eiji; Radhakrishnan; Yamamoto, Yoshinori
Journal of the American Chemical Society, 2000 , vol. 122, # 30 p. 7280 - 7286
反应条件
2,6-dimethylpyridine; water; cesium fluoride in acetonitrile T=70°C; 12 h;
参考文献
Lee, Yi-Hsien; Chen, Yen-Chung; Hsieh, Jen-Chieh
European Journal of Organic Chemistry, 2012 , # 2 p. 247 - 250
反应条件
cesium fluoride in acetonitrile T=0 - 20°C;
参考文献
Kolomeitsev, Alexander A.; Vorobyev, Mikhail; Gillandt, Hartmut
Tetrahedron Letters, 2008 , vol. 49, # 3 p. 449 - 454
反应条件
potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=20°C; 4 h;
参考文献
Chemical Communications, , # 15 p. 1505 - 1507
反应条件
cesium fluoride in acetonitrile T=20°C; 24 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
2,2,6,6-tetramethyl-piperidine; 1-iodophenylacetylene; cesium fluoride in acetonitrile T=50°C; 5 h; Reagent/catalyst; regioselective reaction;
参考文献
Zeng, Yuwen; Zhang, Laijun; Zhao, Yanchuan; Ni, Chuanfa; Zhao, Jingwei; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 8 p. 2955 - 2958
反应条件
potassium fluoride; 18-crown-6 ether in tetrahydrofuran T=20°C; 24 h;
参考文献
Jin, Tienan; Yang, Fan; Yamamoto, Yoshinori
Collection of Czechoslovak Chemical Communications, 2009 , vol. 74, # 6 p. 957 - 972
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-78 - 20°C; 20 h;
参考文献
Liu, Zhijian; Shi, Feng; Martinez, Pablo D. G.; Raminelli, Cristiano; Larock, Richard C.
Journal of Organic Chemistry, 2008 , vol. 73, # 1 p. 219 - 226
反应条件
cesium fluoride in tetrahydrofuran T=65°C; 24 h;
参考文献
Dubrovskiy, Anton V.; Larock, Richard C.
Tetrahedron, 2013 , vol. 69, # 13 p. 2789 - 2798
反应条件
cesium fluoride in tetrahydrofuran T=125°C; 24 h;
参考文献
Dubrovskiy, Anton V.; Larock, Richard C.
Tetrahedron, 2013 , vol. 69, # 13 p. 2789 - 2798
