2-(三甲基硅)苯基三氟甲烷磺酸盐合成路线 (共 525 条)
反应条件
in diethyl ether; acetonitrile T=0 - 20°C; Title compound not separated from byproducts.;
参考文献
Kolomeitsev, Alexander A.; Vorobyev, Mikhail; Gillandt, Hartmut
Tetrahedron Letters, 2008 , vol. 49, # 3 p. 449 - 454
反应条件
potassium fluoride; 18-crown-6 ether; 3-(2,4,6-trimethyl-phenyl)-5,6,7,8-tetrahydro-4H-cycloheptathiazol-3-ium perchlorate; potassium tert-butylate in tetrahydrofuran T=25°C; 4 h; Inert atmosphere;
参考文献
Biju, Akkattu T.; Glorius, Frank
Angewandte Chemie - International Edition, 2010 , vol. 49, # 50 p. 9761 - 9764
反应条件
cesium fluoride in acetonitrile T=20°C; 10 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 8 p. 3198 - 3209
反应条件
cesium fluoride in acetonitrile T=20°C; 5 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
potassium fluoride T=80°C; 5 h; Inert atmosphere;
参考文献
Yoshida, Hiroto; Ito, Yu; Ohshita, Joji
Chemical Communications, 2011 , vol. 47, # 30 p. 8512 - 8514
反应条件
1: 2-butyl furan; sodium hydroxide / acetonitrile / 5 h / 20 °C / Inert atmosphere 2: 18-crown-6 ether; nonafluoro-n-butanesulfonyl fluoride; caesium carbonate / acetonitrile / 2 h / 60 °C / Inert atmosphere View Scheme
参考文献
Ikawa, Takashi; Nishiyama, Tsuyoshi; Nosaki, Toshifumi; Takagi, Akira; Akai, Shuji
Organic Letters, 2011 , vol. 13, # 7 p. 1730 - 1733
反应条件
cesium fluoride in acetonitrile T=20°C; 72 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
2,6-dimethylpyridine; water; cesium fluoride in acetonitrile T=70°C; 12 h;
参考文献
Lee, Yi-Hsien; Chen, Yen-Chung; Hsieh, Jen-Chieh
European Journal of Organic Chemistry, 2012 , # 2 p. 247 - 250
反应条件
cesium fluoride in acetonitrile T=20°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 8 p. 3198 - 3209
反应条件
cesium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in acetonitrile T=80°C; Elimination; Cyclization; 3 h; Title compound not separated from byproducts;
参考文献
Yoshikawa, Eiji; Radhakrishnan; Yamamoto, Yoshinori
Journal of the American Chemical Society, 2000 , vol. 122, # 30 p. 7280 - 7286