2-(三甲基硅)苯基三氟甲烷磺酸盐合成路线 (共 525 条)
反应条件
1: 2-bromophenyl trimethylsilyl ether With n-butyllithium in diethyl ether T=20°C; 0.0166667 h; Flow reactor; 2: trifluoromethylsulfonic anhydride in diethyl ether T=20°C; 0.00202778 h; Flow reactor;
参考文献
Michel, Boris; Greaney, Michael F.
Organic Letters, 2014 , vol. 16, # 10 p. 2684 - 2687
反应条件
pyridine in dichloromethane T=0°C; Inert atmosphere;
参考文献
Atkinson, Darcy J.; Sperry, Jonathan; Brimble, Margaret A.
Synthesis, 2010 , # 6 p. 911 - 913
反应条件
in acetonitrile T=23°C; 2.33333 h; Inert atmosphere;
参考文献
Bronner, Sarah M.; Garg, Neil K.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8842 - 8843
反应条件
n-butyllithium 1.) Et2O, 0 deg C to RT, 4 h; 2.) Et2O, 0 deg C to RT; Yield given. Multistep reaction;
参考文献
Chemistry Letters, , p. 1211 - 1214
反应条件
potassium fluoride T=80°C; 8.5 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 30 p. 8512 - 8514
反应条件
cesium fluoride in acetonitrile T=20°C; 72 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; cesium fluoride; bis(dibenzylideneacetone)-palladium(0) in toluene; acetonitrile T=110°C; 24 h; ConcentrationReagent/catalystSolventTemperatureTime;
参考文献
Lu, Chun; Markina, Nataliya A.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 24 p. 11153 - 11160
反应条件
cesium fluoride in acetonitrile T=20°C; 72 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 8 p. 3198 - 3209
反应条件
cesium fluoride in acetonitrile T=20°C; 10 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 8 p. 3198 - 3209
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-78 - 20°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 1 p. 219 - 226