1: 52 percent / pyridine / 12 h
2: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
3: 39 percent / H2O / 0.17 h / Heating
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 52 percent / pyridine / 12 h
2: 53 percent / PCl5 / CH2Cl2 / 0.08 h
3: 54 percent / Et3N / CH2Cl2 / 12 h
4: 50 percent / potassium t-butoxide / tetrahydrofuran / 1 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 52 percent / pyridine / 12 h
2: 53 percent / PCl5 / CH2Cl2 / 0.08 h
3: 59 percent / Et3N / CH2Cl2 / 12 h
4: 22 percent / potassium t-butoxide / tetrahydrofuran / 1 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 52 percent / pyridine / 12 h
2: 53 percent / PCl5 / CH2Cl2 / 0.08 h
3: 59 percent / Et3N / CH2Cl2 / 12 h
4: 22 percent / potassium t-butoxide / tetrahydrofuran / 1 h / 0 °C
5: 40 percent / tetrahydrofuran / 1 h
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 92 percent / Et3N / CH2Cl2 / 18 h
2: 65 percent / NaH / dimethylformamide / 1 h / 0 °C
3: 46 percent / 1M hydrochloric acid / acetone / 1 h
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
1: 52 percent / pyridine / 12 h
2: 77 percent / NaH / dimethylformamide / 0.75 h / 0 °C
View Scheme
参考文献
Al-Zaidi, Shakir M.R.; Crilley, Martine M. L.; Stoodley, Richard J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2259 - 2266
