2-(呋喃-2-基)苯并[d]噁唑合成路线 (共 24 条)
反应条件
1: ethanol / Heating
2: methylcyclohexane / Ambient temperature; Irradiation
View Scheme
参考文献
Tauer, Erich; Grellmann, Karl H.
Journal of Organic Chemistry, 1981 , vol. 46, # 21 p. 4252 - 4258
反应条件
in 1-methyl-pyrrolidin-2-one
2 h; Reflux;
参考文献
Aleksandrov; Vlasova; El'Chaninov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 6 p. 898 - 902
反应条件
1: hydrazine / methanol; chloroform; water / 12 h / 20 °C
2: acetic acid / water / 0.5 h / 20 °C
3: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3.5 h / 80 °C
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参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: acetic acid / water / 0.5 h / 20 °C
2: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3.5 h / 80 °C
View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: pyridine; copper(I) bromide / dichloromethane / 48 h / 20 °C / Molecular sieve
2: hydrazine / methanol; chloroform; water / 12 h / 20 °C
3: acetic acid / water / 0.5 h / 20 °C
4: oxygen; copper(II) bis(trifluoromethanesulfonate) / toluene / 3.5 h / 80 °C
View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Raiford; Huey
Journal of Organic Chemistry, 1941 , vol. 6, p. 858,865
反应条件
1: water
2: SnCl2; concentrated aqueous HCl
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参考文献
Raiford; Huey
Journal of Organic Chemistry, 1941 , vol. 6, p. 858,865
反应条件
1: water
2: SnCl2; concentrated aqueous HCl
View Scheme
参考文献
Raiford; Huey
Journal of Organic Chemistry, 1941 , vol. 6, p. 858,865
反应条件
T=700°C; P=0.01 Torr; 1 h; flash vacuum pyrolysis;
参考文献
Chou, Chin-Hsing; Hsueh, Yu-Tan; Wang, Bo-Chi
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 3 p. 301 - 305
反应条件
in 2-methyl cyclohexane
Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Tauer, Erich; Grellmann, Karl H.
Journal of Organic Chemistry, 1981 , vol. 46, # 21 p. 4252 - 4258