2-(3,4-二氢异喹啉-2(1H)-基)乙醇合成路线 （共 15 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
3 h; Heating;
参考文献
Ferles, Miloslav; Silhankova, Alexandra; Kafka, Stanislav; Taufmann, Petr; Motacek, Tomas
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # l p. 1759 - 1764
反应条件
1: With naphthalene; potassium in tetrahydrofuran
T=-30°C; 5 h;
2: With water in tetrahydrofuran
T=-30°C; 0.5 h;
参考文献
Azzena, Ugo; Pisano, Luisa; Pittalis, Mario
Heterocycles, 2004 , vol. 63, # 2 p. 401 - 409
参考文献
Anderson; Belelli; Bennett; Buchanan; Casula; Cooke; Feilden; Gemmell; Hamilton; Hutchinson; Lambert; Maidment; McGuire; McPhail; Miller; Muntoni; Peters; Sansbury; Stevenson; Sundaramt
Journal of Medicinal Chemistry, 2001 , vol. 44, # 22 p. 3582 - 3591
反应条件
1: 95 percent / benzene / 240 h
2: 56 percent / NaBH4 / ethanol / 2.5 h
3: 54.5 percent / 75percent LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Ferles, Miloslav; Silhankova, Alexandra; Kafka, Stanislav; Taufmann, Petr; Motacek, Tomas
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # l p. 1759 - 1764
反应条件
sodium tetrahydroborate in methanol
1 h; Yield given;
参考文献
Moehrle; Tot; Steiner
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 8 p. 711 - 717
反应条件
chloroform
T=40 - 60°C; im Rohr;
参考文献
v. Braun; Braunsdorf; Raeth
Chemische Berichte, 1922 , vol. 55, p. 1679
参考文献
Lukevits; Segal; Zablotskaya; Germane
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 6 p. 682 - 688
反应条件
hydrogenchloride; tin
参考文献
Slomka; Schueler
Journal of the American Pharmaceutical Association (1912-1977), 1951 , vol. 40, p. 47,49
参考文献
Zablotskaya, Alla; Segal, Izolda; Popelis, Yuris; Grinberga, Solveiga; Shestakova, Irina; Nikolajeva, Vizma; Eze, Daina
Applied Organometallic Chemistry, 2013 , vol. 27, # 2 p. 114 - 124
参考文献
Skita
Chemische Berichte, 1924 , vol. 57, p. 1980
