3,5-二叔丁基-4-羟基苄醇合成路线 (共 55 条)
反应条件
nitric acid; sodium nitrite
T=-20°C;
参考文献
Bozell, Joseph J.; Hoberg, John O.; Dimmel, Donald R.
Tetrahedron Letters, 1998 , vol. 39, # 16 p. 2261 - 2264
反应条件
1: 98 percent / laccase; oxygen; TEMPO / acidic aq. solution / 24 h / 20 °C / pH 5
2: t-BuOK / acetonitrile / 36 h / 80 °C
3: NaBH4; NaOH / propan-2-ol
View Scheme
参考文献
D'Acunzo, Francesca; Galli, Carlo; Gentili, Patrizia; Sergi, Federica
New Journal of Chemistry, 2006 , vol. 30, # 4 p. 583 - 591
反应条件
pyridine; p-toluenesulfonyl chloride
参考文献
Teubner,H.-J. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 757 - 770
反应条件
hydrogenchloride in dichloromethane
6 h; Ambient temperature;
参考文献
De Caro, Pascale Satge; Mouloungui, Zephirin; Gaset, Antoine
JAOCS, Journal of the American Oil Chemists' Society, 1997 , vol. 74, # 3 p. 241 - 247
参考文献
Koutek,B. et al.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 2250 - 2255