N,N-二乙基氯甲酰胺合成路线 (共 193 条)
反应条件
1: With chlorine in dichloromethane T=24 - 26°C; 7 h; Cooling with ice; 2: With water; sodium hydrogencarbonate in dichloromethane Cooling with ice;
参考文献
Adeppa; Rupainwar; Misra, Krishna
Synthetic Communications, 2011 , vol. 41, # 2 p. 285 - 290
反应条件
1: in dichloromethane T=40°C; Inert atmosphere; 2: With chlorine in dichloromethane T=20°C;
参考文献
Adeppa; Rupainwar; Misra, Krishna
Canadian Journal of Chemistry, 2010 , vol. 88, # 12 p. 1277 - 1280
反应条件
sodium hydrogencarbonate in dichloromethane T=-10°C;
参考文献
Yuan, Wen; Shang, Zhipei; Qiang, Xiaoming; Tan, Zhenghuai; Deng, Yong
Research on Chemical Intermediates, 2014 , vol. 40, # 2 p. 787 - 800
反应条件
sulfuryl dichloride T=0 - 20°C; 1 h;
参考文献
Mizuno, Takumi; Takahashi, Junko; Ogawa, Akiya
Tetrahedron, 2003 , vol. 59, # 8 p. 1327 - 1331
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 31, p. 691
反应条件
trichlorophosphate in acetonitrile 7 h; Heating;
参考文献
Hoshino, Osamu; Saito, Keiji; Ishizaki, Miyuki; Umezawa, Bunsuke
Synthetic Communications, 1987 , vol. 17, # 16 p. 1887 - 1892
反应条件
sulfuryl dichloride in benzene T=50°C; 6 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 4.2 p. 819 - 822
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 909 - 913
反应条件
in dichloromethane T=0°C;
参考文献
Organic Letters, , vol. 14, # 14 p. 3676 - 3679
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 44, p. S128 - S131
反应条件
in 1,4-dioxane T=55 - 60°C; 4 h;
参考文献
Journal of Pharmaceutical Sciences, , vol. 80, # 8 p. 793 - 798