2,4,6-三甲基苯胺合成路线 （共 254 条）
参考文献
Maisse-Franois, Aline; Azor, Laurine; Schmitt, Anne-Laure; Coquel, Ariane; Brelot, Lydia; Welter, Richard; Bellemin-Laponnaz, Stephane; Dagorne, Samuel
Journal of Organometallic Chemistry, 2012 , vol. 696, # 26 p. 4248 - 4256
反应条件
in isopropyl alcohol; benzene
Heating;
参考文献
Goyal; Singh
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2001 , vol. 40, # 6 p. 638 - 641
反应条件
1: 70 percent / benzene / 2 h / Heating
2: 75 percent / CH3COCl / 6 h / Heating
3: 65 percent / sodium acetate / acetic acid / 8 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 714 - 716
反应条件
1: 70 percent / benzene / 2 h / Heating
2: 75 percent / CH3COCl / 6 h / Heating
3: 60 percent / sodium acetate / acetic acid / 8 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 714 - 716
反应条件
1: 70 percent / benzene / 2 h / Heating
2: 75 percent / CH3COCl / 6 h / Heating
3: 60 percent / sodium acetate / acetic acid / 8 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 714 - 716
反应条件
1: 55 percent / benzene / 2 h / Heating
2: 55 percent / CH3COCl / 6 h / Heating
3: 60 percent / sodium acetate / acetic acid / 8 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 714 - 716
反应条件
sodium hydride
1.) 1,4-dioxane, 100 deg C, 2 h, 2.) 1,4-dioxane, 100 deg C, 2 h; Multistep reaction;
参考文献
Miyano, Seiji; Sumoto, Kunihiro; Satoh, Fumio; Shima, Keiyu; Hayashimatsu, Mariko; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 6 p. 714 - 717
反应条件
1: 85 percent / formic acid (90percent), acetic anhydride / 3 h / Heating
2: NaOH, zinc dust / H2O; ethanol / 1 h / Heating
View Scheme
参考文献
Goldstein, Stephen L.; McNelis, Edward
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1613 - 1620
反应条件
tris-(dibenzylideneacetone)dipalladium(0); BI-DIME; sodium t-butanolate in toluene
T=110°C; Inert atmosphere;
参考文献
Rodriguez, Sonia; Qu, Bo; Haddad, Nizar; Reeves, Diana C.; Tang, Wenjun; Lee, Heewon; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 533 - 537
反应条件
1: With trichlorophosphate
Heating;
2: With water
参考文献
Hirashima, Akinori; Morimoto, Masako; Kuwano, Eiichi; Taniguchi, Eiji; Eto, Morifusa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 117 - 123
