4-(三氟甲氧基)-4’-氯苯甲酮合成路线 （共 5 条）
反应条件
hydrogen fluoride; boron trifluoride T=10°C; 3 h;
参考文献
Desbois, Michel
Bulletin de la Societe Chimique de France, 1986 , # 6 p. 885 - 890
反应条件
hydrogen fluoride; boron trifluoride in dichloromethane T=-5 - -1°C; Acylation; Friedel-Crafts reaction; P=7500.6 Torr; 40 h;
参考文献
Karrer, Friedrich; Meier, Hans; Pascual, Alfons
Journal of Fluorine Chemistry, 2000 , vol. 103, # 1 p. 81 - 84
反应条件
in diethyl ether Grignard reaction; Heating;
参考文献
Boeger, Manfred; Duerr, Dieter; Gsell, Laurenz; Hall, Roger G.; Karrer, Friedrich; Kristiansen, Odd; Maienfisch, Peter; Pascual, Alfons; Rindlisbacher, Alfred
Pest Management Science, 2001 , vol. 57, # 2 p. 191 - 202
反应条件
1: HF / 18 h / -25 - 20 °C 2: HF; BF3 / CH2Cl2 / 40 h / -5 - -1 °C / 7500.6 Torr View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 103, # 1 p. 81 - 84
反应条件
1: 92 percent / Cl2; PCl5 / 200 °C 2: HF / 18 h / -25 - 20 °C 3: HF; BF3 / CH2Cl2 / 40 h / -5 - -1 °C / 7500.6 Torr View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 103, # 1 p. 81 - 84
