β-(二甲氨基)苯丙酮 盐酸盐合成路线 (共 71 条)
反应条件
in ethanol 24 h; Ambient temperature;
参考文献
Holxgrabe, Ulrike
Archiv der Pharmazie (Weinheim, Germany), 1989 , vol. 322, p. 137 - 140
反应条件
in ethanol; water
1 h; Reflux;
参考文献
Roman, Gheorghe
Central European Journal of Chemistry, 2012 , vol. 10, # 5 p. 1516 - 1526,11
Title/Abstract Full Text Show Details
Roman, Gheorghe
Central European Journal of Chemistry, 2012 , vol. 10, # 5 p. 1516 - 1526
反应条件
dichloro bis(acetonitrile) palladium(II) in acetonitrile
6 h; Heating;
参考文献
Murahashi, Shun-Ichi; Mitsue, Yo; Tsumiyama, Tatsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3285 - 3290
反应条件
dichloro bis(acetonitrile) palladium(II); sodium carbonate in acetonitrile
12 h; Heatingdifferent β-amino ketones, bases, solvents and reaction times; Product distribution;
参考文献
Murahashi, Shun-Ichi; Mitsue, Yo; Tsumiyama, Tatsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3285 - 3290
反应条件
in 1,4-dioxane
16 h; Heating;
参考文献
Sielemann, Dirk; Keuper, Ralf; Risch, Nikolaus
Advanced Synthesis and Catalysis, 1999 , vol. 341, # 5 p. 487 - 491
反应条件
triethylamine
T=160°C; 0.333333 h;
参考文献
Zhuo, Jin-Cong; Schenk, Kurt
Helvetica Chimica Acta, 2002 , vol. 85, # 5 p. 1276 - 1283
反应条件
1: 97 percent / aq. NaOH / H2O / 0 - 5 °C / pH 10
2: 0.5 h / 155 °C
View Scheme
参考文献
Surya Prakash Rao; Jeyalakshmi; Senthilkumar
Tetrahedron, 2002 , vol. 58, # 11 p. 2189 - 2199
反应条件
in 1,4-dioxane
16 h; RefluxInert atmosphereSchlenk technique;
参考文献
Kourkoulos, Dimitrios; Karakus, Cueneyt; Hertel, Dirk; Alle, Ronald; Schmeding, Sebastian; Hummel, Johanna; Risch, Nikolaus; Holder, Elisabeth; Meerholz, Klaus
Dalton Transactions, 2013 , vol. 42, # 37 p. 13612 - 13621
反应条件
in various solvent(s)
Michael addition; 0.0333333 h; microwave irradiation;
参考文献
Rao, H. Surya Prakash; Poonguzhali; Senthilkumar
Synthetic Communications, 2008 , vol. 38, # 6 p. 937 - 942
反应条件
in ethanol
1 h; Heating;
参考文献
Borisova, E. Ya.; Sitsun', Van; Moskovkin, A. S.; Golovkov, P. V.; Tubashova, I. A.; Cherkashin, M. I.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 11.2 p. 1871 - 1875
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 11 p. 2255 - 2259