β-(二甲氨基)苯丙酮 盐酸盐合成路线 (共 71 条)
反应条件
sodium hydroxide; sodium hypochlorite in water 3 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
反应条件
hydrogenchloride; sodium carbonate 1.) N,N-dimethylformamide, 6 h; 2.) ether;
参考文献
Occelli, E.; Fontanella, L.; Diena, A.; Schiatti, P.
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 2 p. 86 - 101
反应条件
sodium hydroxide; sodium hypochlorite in water 3 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
反应条件
sodium hydroxide; sodium hypochlorite in water 3 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 69, # 12 p. 1904 - 1908
反应条件
triethylamine in ethanol 2 h; Heating;
参考文献
Eichinger; Nussbaumer
Synthesis, 1991 , # 8 p. 663 - 664
反应条件
bei der Wasserdampfdestillation;
参考文献
Mannich; Heilner
Chemische Berichte, 1922 , vol. 55, p. 362
反应条件
1: 81 percent / PdCl2(MeCN)2, triethylamine / acetonitrile / 12 h / Heating 2: 1.) CuI / 1.) ether, RT, 15 min; 2.) ether, RT, overnight View Scheme
参考文献
Murahashi, Shun-Ichi; Mitsue, Yo; Tsumiyama, Tatsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3285 - 3290
反应条件
in ethanol Cyclocondensation; 12 h; Heating;
参考文献
Graef, Edgar; Troschuetz, Reinhard
Synthesis, 1999 , # 7 p. 1216 - 1222
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol; water T=100°C; 1.5 h;
参考文献
Occelli, E.; Fontanella, L.; Diena, A.; Schiatti, P.
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 2 p. 86 - 101
参考文献
Tilak, B. D.; Gogte, V.N.; Modak, A.S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 414 - 415