β-(二甲氨基)苯丙酮 盐酸盐合成路线 （共 71 条）
反应条件
hydrogenchloride in water; isopropyl alcohol T=80 - 85°C; 5 h;
参考文献
IND-SWIFT LABORATORIES LIMITED
Patent: WO2009/141833 A2, 2009 ;
Location in patent: Page/Page column 11 ;
反应条件
hydrogenchloride T=90°C; 3.5 h;
参考文献
Sumita; Koumori; Ohno
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 8 p. 1676 - 1678
反应条件
hydrogenchloride; paraformaldehyde in ethanol
参考文献
Fujiwara, Junya; Sakai, Kazuya; Kibayashi, Kenji; Shimada, Fumiki; Shiga, Yoshio; Takagi, Shiro
Patent: US2003/149046 A1, 2003 ;
反应条件
in acetonitrile 1 h; Heating;
参考文献
Kaiser, Stefan; Smidt, Sebastian P.; Pfaltz, Andreas
Angewandte Chemie - International Edition, 2006 , vol. 45, # 31 p. 5194 - 5197
反应条件
hydrogenchloride; paraformaldehyde in ethanol; acetone
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; oxygen in dimethyl sulfoxide 3 h;
参考文献
Donetti, Arturo; Boniardi, Orazio; Ezhaya, Antoine
Synthesis, 1980 , # 12 p. 1009 - 1011
反应条件
water Mannich reaction; 0.0138889 h; combined microwave and ultrasound irradiation;
参考文献
Peng, Yanqing; Dou, Ruiling; Song, Gonghua; Jiang, Jun
Synlett, 2005 , # 14 art. no. U19205ST, p. 2245 - 2247
反应条件
hydrogenchloride in ethanol T=60°C; Mannich reaction;
参考文献
Heterocyclic Communications, , vol. 11, # 2 p. 135 - 138
反应条件
1: 81 percent / PdCl2(MeCN)2, triethylamine / acetonitrile / 12 h / Heating 2: 1.) CuI / 1.) ether, RT, 15 min; 2.) ether, RT, overnight View Scheme
参考文献
Murahashi, Shun-Ichi; Mitsue, Yo; Tsumiyama, Tatsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3285 - 3290
反应条件
sodium hydroxide in water T=0 - 5°C; pH=10;
参考文献
Surya Prakash Rao; Jeyalakshmi; Senthilkumar
Tetrahedron, 2002 , vol. 58, # 11 p. 2189 - 2199
