3-乙酰氧基-3-甲基戊烷-1,5-二酸酸酸酐合成路线 (共 11 条)
参考文献
Ahmed, Salman A.; Bardshiri, Esfandiar; McIntyre, C. Rupert; Simpson, Thomas J.
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 249 - 274
反应条件
1: aqueous alkali 2: acetic acid anhydride; benzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 2377
反应条件
1: 1.) O3, HOAc; 2.) H2O2, HOAc / 1.) CH2Cl2 2: Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 883 - 884
参考文献
Bardshiri, Esfandiar; Simpson, Thomas J.; Scott, A. Ian; Shishido, Kozo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 8 p. 1765 - 1767
反应条件
1: xylene / Heating 3: 2.) Ag2O, MgSO4 / 1.) xylene, reflux 4: HBr, HOAc View Scheme
参考文献
Ahmed, Salman A.; Bardshiri, Esfandiar; McIntyre, C. Rupert; Simpson, Thomas J.
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 249 - 274
反应条件
1: 100 percent / xylene / 20 h / Heating 2: 83 percent / diethyl ether / 1 h / Ambient temperature 3: 2.) Ag2O, MgSO4 / 1.) xylene, reflux, 5 d, 2.) xylene, RT, 12 h 4: 100 percent / 48percent HBr / acetic acid / 5 h / Heating View Scheme
参考文献
Ahmed, Salman A.; Bardshiri, Esfandiar; Simpson, Thomas J.
Journal of the Chemical Society, Chemical Communications, 1987 , p. 883 - 884
反应条件
sodium tetrahydroborate in isopropyl alcohol 24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1417 - 1420
反应条件
sodium tetrahydroborate in isopropyl alcohol
24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Lewer, Paul; MacMillan, Jake
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 7 p. 1417 - 1420
反应条件
sodium tetrahydroborate in isopropyl alcohol
24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Lewer, Paul; MacMillan, Jake
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 7 p. 1417 - 1420
反应条件
in xylene
20 h; Heating;
参考文献
Ahmed, Salman A.; Bardshiri, Esfandiar; McIntyre, C. Rupert; Simpson, Thomas J.
Australian Journal of Chemistry, 1992 , vol. 45, # 1 p. 249 - 274