(3-羟基甲基吡啶-2-基)氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran; methanol T=0 - 20°C; 4 h; 2: With water; sodium hydrogencarbonate in tetrahydrofuran; methanol; ethyl acetate
参考文献
WO2006/106326 A1, ;
Page/Page column 129-130 ;
WO 2006/106326 A1
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C;
参考文献
Krasavin, Mikhail; Shkavrov, Sergey; Kravchenko, Dmitry
Synthetic Communications, 2006 , vol. 36, # 2 p. 181 - 186
反应条件
1: 55 percent / sulfuric acid / 20 h / Heating 2: 75 percent / 4-(dimethylamino)pyridine / CH2Cl2 / 36 h / 20 °C 3: 65 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 36, # 2 p. 181 - 186
反应条件
1: 75 percent / 4-(dimethylamino)pyridine / CH2Cl2 / 36 h / 20 °C 2: 65 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 36, # 2 p. 181 - 186
