(±)-反式-1,3-二苯基烯丙基乙酸酯合成路线 （共 31 条）
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran T=50°C; 19 h;
参考文献
Bower, Justin F.; Jumnah, Roshan; Williams, Andrew C.; Williams, Jonathan M. J.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 9 p. 1411 - 1420
反应条件
chiral (S)-proline-phosphine-oxazoline ligand; [Pd2(dba)2] in tetrahydrofuran T=0°C; 12 h;
参考文献
Chen, Junmin; Lang, Feng; Li, Dong; Cun, Linfeng; Zhu, Jin; Deng, Jingen; Liao, Jian
Tetrahedron Asymmetry, 2009 , vol. 20, # 17 p. 1953 - 1956
反应条件
tris(dibenzylideneacetone)dipalladium (0); (R)-2-(N,N-diisopropylcarbamoyloxy)-2'-diphenylphosphino-1,1'-binaphthyl in tetrahydrofuran T=50°C; Substitution; 48 h; Title compound not separated from byproducts;
参考文献
Ohta, Tetsuo; Sasayama, Hiroyuki; Nakajima, Osakazu; Kurahashi, Nobukazu; Fujii, Takeshi; Furukawa, Isao
Tetrahedron Asymmetry, 2003 , vol. 14, # 5 p. 537 - 542
反应条件
1: rac-(E)-1,3-diphenylprop-2-en-1-yl acetate With bis(η3-allyl-μ-chloropalladium(II)); C47H50FeN3OP2(1+)*F6P(1-) in dichloromethane T=20°C; 0.25 h; Ionic liquidInert atmosphere; 2: phthalimide With potassium acetate; N,N-bis(trimethylsilyl)acetamide in dichloromethane T=20°C; 48 h; Ionic liquidInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Sebesta, Radovan; Bilcik, Filip
Tetrahedron Asymmetry, 2009 , vol. 20, # 16 p. 1892 - 1896
反应条件
1: bis(η3-allyl-μ-chloropalladium(II)); C42H51O6PS; caesium carbonate / dichloromethane / 12 h / 23 °C / |Schlenk technique; |Inert atmosphere 2: Grubb's 2nd generation catalyst / dichloromethane / 16 h / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Coll, Merce; Pamies, Oscar; Dieguez, Montserrat
Organic Letters, 2014 , vol. 16, # 7 p. 1892 - 1895
反应条件
potassium phosphate; triphenylphosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in water; toluene T=170°C; 0.025 h; microwave irradiation;
参考文献
Polackova, Viera; Toma, Stefan; Oliver Kappe
Tetrahedron, 2007 , vol. 63, # 36 p. 8742 - 8745
反应条件
pyridine
1 h; Heating;
参考文献
Watson, Iain D. G.; Styler, Sarah A.; Yudin, Andrei K.
Journal of the American Chemical Society, 2004 , vol. 126, # 16 p. 5086 - 5087
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Watson, Iain D. G.; Yudin, Andrei K.
Journal of the American Chemical Society, 2005 , vol. 127, # 49 p. 17516 - 17529
反应条件
air; palladium diacetate; silver carbonate in benzene
Heck reaction; 15 h; Reflux; stereoselective reaction;
参考文献
Pan, Delin; Chen, Anjun; Su, Yijin; Zhou, Wang; Li, Si; Jia, Wei; Xiao, Juan; Liu, Qingjian; Zhang, Liangren; Jiao, Ning
Angewandte Chemie - International Edition, 2008 , vol. 47, # 25 p. 4729 - 4732
反应条件
Y5(OiPr)13O
T=20°C; Acetylation; transesterification; 1.5 h;
参考文献
Lin, Mei-Huey; RajanBabu
Organic Letters, 2000 , vol. 2, # 7 p. 997 - 1000
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in diethyl ether
T=20°C; 12 h;
参考文献
Faller; Wilt, Jeremy C.; Parr, Jonathan
Organic Letters, 2004 , vol. 6, # 8 p. 1301 - 1304
