2,4,6-三甲氧基-1,3,5-三嗪合成路线 (共 31 条)
反应条件
sodium methylate in methanol; diethyl ether
反应条件
methanol in tetrahydrofuran room temp. in the presence of K2CO3 as HCl-acceptor;
参考文献
Grisley et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 1802
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 7.1.4.3, page 272 - 272
反应条件
sodium hydroxide T=20°C; 2 h;
参考文献
Nedel'ko; Shastin; Korsunskii; Chukanov; Larikova; Kazakov
Russian Chemical Bulletin, 2005 , vol. 54, # 7 p. 1710 - 1714
反应条件
in methanol T=-5 - 20°C; Heating / reflux;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1201658 A1, 2002 ;
Location in patent: Example 8 ;
反应条件
in toluene Substitution; 3 h;
参考文献
Tripolt, Robert; Schmuck, Siegfried; Nachbaur, Edgar
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1999 , vol. 54, # 5 p. 609 - 616
反应条件
sodium 1 h; Ambient temperature;
参考文献
Shastin, A. V.; Godovikova, T. I.; Golova, S. P.; Khmel'nitskii, L. I.; Korsunskii, B. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1995 , vol. 31, # 5 p. 596 - 600
Khimiya Geterotsiklicheskikh Soedinenii, 1995 , # 5 p. 674 - 678
反应条件
1: in water 0.333333 h; 2: in water T=120°C; 72 h;
参考文献
Cao, Qiang
Journal of Chemical Research, 2012 , vol. 36, # 11 p. 648 - 651
反应条件
acetic acid T=20°C; 10 h;
参考文献
Synthesis, , # 4 p. 542 - 544
反应条件
(Ph3P)2Pd(N3)2 in dichloromethane further reagent: (Ph3P)2Pt(N3)2;
参考文献
Chemische Berichte, , vol. 116, # 7 p. 2691 - 2707
反应条件
tetrahydrofuran; potassium carbonate
参考文献
Journal of Organic Chemistry, , vol. 23, p. 1802