4-(苄氧基)-3-羟基苯甲酸甲酯合成路线 （共 6 条）
反应条件
potassium carbonate in acetone
T=20°C; 48 h;
参考文献
Desroses, Matthieu; Laconde, Guillaume; Depreux, Patrick; Henichart, Jean-Pierre
Organic Preparations and Procedures International, 2004 , vol. 36, # 5 p. 445 - 452
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 20°C; Mitsunobu reaction; regioselective reaction;
参考文献
Wang, Xiaolong; Ju, Tingting; Li, Xiaodong; Cao, Xiaoping
Synlett, 2010 , # 19 p. 2947 - 2949
反应条件
potassium carbonate in acetonitrile
24 h; Heating;
参考文献
He, Chunlin; Shi, Zuming; Zhou, Qizhong; Li, Shijun; Li, Ning; Huang, Feihe
Journal of Organic Chemistry, 2008 , vol. 73, # 15 p. 5872 - 5880
反应条件
1.1: 85 percent / p-TsOH / 72 h / Heating
2.1: K2CO3 / acetonitrile / 4 h / 85 °C
2.2: 51 percent / acetonitrile / 12 h / 65 °C
View Scheme
参考文献
Gibson, Harry W.; Wang, Hong; Bonrad, Klaus; Jones, Jason W.; Slebodnick, Carla; Zackharov, Lev N.; Rheingold, Arnold L.; Habenicht, Bradley; Lobue, Peter; Ratliff, Amy E.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 11 p. 2114 - 2121
参考文献
Canonica et al.
Annali di Chimica (Rome, Italy), 1956 , vol. 46, p. 465,473
反应条件
1: 96 percent / K2CO3 / acetone / 5 h / Heating
2: 94 percent / H2 / Pd/C / methanol / 48 h / 20 °C
View Scheme
参考文献
Desroses, Matthieu; Laconde, Guillaume; Depreux, Patrick; Henichart, Jean-Pierre
Organic Preparations and Procedures International, 2004 , vol. 36, # 5 p. 445 - 452
