反应条件
1: H2 / 5percent palladium on charcoal / ethanol / 16 h / Ambient temperature
2: tert-butyl hypochlorite / diethyl ether / 0.5 h / 0 °C
3: sodium ethoxide / ethanol / 1 h / 40 °C
4: 5percent sulfuric acid / H2O / 2 h / Ambient temperature
5: 86 percent / 10percent NaOH / H2O / 2 h / 0 °C
View Scheme
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894