2-(二甲氧基甲基)苯甲酸甲酯合成路线 （共 10 条）
反应条件
hydrogenchloride in methanol
参考文献
Wang, Le; Shen, Wang
Tetrahedron Letters, 1998 , vol. 39, # 42 p. 7625 - 7628
反应条件
1: 83 percent / LAH / diethyl ether / 12 h / Ambient temperature 2: 55 percent / acetic acid; H2O / 12 h / 100 °C View Scheme
参考文献
Smith, James G.; Dibble, Peter W.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5361 - 5362
反应条件
1: 83 percent / LAH / diethyl ether / 12 h / Ambient temperature 2: 25 percent / acetic acid; H2O / 10 h / 100 °C View Scheme
参考文献
Smith, James G.; Dibble, Peter W.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5361 - 5362
反应条件
1: 83 percent / LAH / diethyl ether / 12 h / Ambient temperature 2: 70 percent / acetic acid; H2O / 12 h / 100 °C View Scheme
参考文献
Smith, James G.; Dibble, Peter W.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5361 - 5362
反应条件
Dowex 50W-X8 resin; trimethyl orthoformate
15 h; Heating;
参考文献
Smith, James G.; Dibble, Peter W.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5361 - 5362
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride
P=20685.9 Torr;
参考文献
Wang, Le; Shen, Wang
Tetrahedron Letters, 1998 , vol. 39, # 42 p. 7625 - 7628
反应条件
1: Et3N
2: PdCl2*dppf / 20685.9 Torr
View Scheme
参考文献
Wang, Le; Shen, Wang
Tetrahedron Letters, 1998 , vol. 39, # 42 p. 7625 - 7628
反应条件
1: 83 percent / LAH / diethyl ether / 12 h / Ambient temperature
2: Dowex 50W-X8 resin / 12 h / Ambient temperature
View Scheme
参考文献
Smith, James G.; Dibble, Peter W.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5361 - 5362
反应条件
lithium aluminium tetrahydride in diethyl ether
12 h; Ambient temperature;
参考文献
Smith, James G.; Dibble, Peter W.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5361 - 5362
反应条件
1: HCl / methanol
2: PPh3
3: 92 percent / tris(dibenzylideneacetone)dipalladium (Pd2(dba)3), tris(2-furyl)phosphine (TFP) / toluene / 20 h / 100 °C
View Scheme
参考文献
Wang, Le; Shen, Wang
Tetrahedron Letters, 1998 , vol. 39, # 42 p. 7625 - 7628
