反应条件
In inert atmosphere, heating of Ru-complex with HSi(Ph2Cl)3 (110°C, 16 h, closed vessel, stirring), periodic pumping to remove PMe3.; Cooling to room temp., addn. of pentane, cooling (-78°C, 6 h), filtn. of pale yellow crystals, washing (pentane, -78°C), drying in vac, elem. anal.;
参考文献
Straus, Daniel A.; Zhang, Cheng; Quimbita, Grace E.; Grumbine, Steven D.; Heyn, Richard H.; Tilley, T. Don; Rheingold, Arnold L.; Geib, Steven J.
Journal of the American Chemical Society, 1990 , vol. 112, # 7 p. 2673 - 2681
