1-环己基亚基丙-2-酮合成路线 (共 41 条)
反应条件
iron; BaO
T=200°C; spaeteres erhitzen auf 320-390grad;
参考文献
Vogel
Journal of the Chemical Society, 1933 , p. 1028,1029
反应条件
2: 1.) O2, tetraphenylporphine, 2.) molecular sieves 4-Angstroem, Ti(O-i-Pr)4 / 1.) CH2Cl2, -10 to -5 deg C, irradiation, 6 h, 2.) 0 deg C, 8 h
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参考文献
Adam, Waldemar; Richter, Markus J.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3341 - 3346
反应条件
titanium(IV) isopropylate; 4 A molecular sieve; oxygen; 5,15,10,20-tetraphenylporphyrin
1.) CH2Cl2, -10 to -5 deg C, irradiation, 6 h, 2.) 0 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Adam, Waldemar; Richter, Markus J.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3341 - 3346
反应条件
diethyl ether; benzene
Zersetzen des Reaktionsprodukts mit Eis unter Durchleiten von Kohlendioxyd;
参考文献
Dickins; Hugh; Kon
Journal of the Chemical Society, 1928 , p. 1635
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Birch; Kon; Norris
Journal of the Chemical Society, 1923 , vol. 123, p. 1365
反应条件
aluminium trichloride
1.) CH2Cl2, 0 deg C, 1 h, 2.) -90 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Laguerre, Michel; Grignon-Dubois, Micheline; Dunogues, Jacques
Tetrahedron, 1981 , vol. 37, p. 1161 - 1169
反应条件
1: thionyl chloride
2: benzene; diethyl ether / Zersetzen des Reaktionsprodukts mit Eis unter Durchleiten von Kohlendioxyd
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参考文献
Birch; Kon; Norris
Journal of the Chemical Society, 1923 , vol. 123, p. 1365
反应条件
sodium ethanolate
Kochen des Reaktionsgemisches mit Wasser;
参考文献
Jupp; Kon; Lockton
Journal of the Chemical Society, 1928 , p. 1642
参考文献
Dickins; Hugh; Kon
Journal of the Chemical Society, 1928 , p. 1635
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Kon; Linstead
Journal of the Chemical Society, 1929 , p. 1275,1277
参考文献
Kon
Journal of the Chemical Society, 1931 , p. 248,251
参考文献
Kon
Journal of the Chemical Society, 1931 , p. 248,251