2,1,3-苯并噻二唑-5-胺合成路线 (共 7 条)
反应条件
stannous chloride in 1,4-dioxane; ethanol; water
参考文献
US6420567 B1, ;
US 6420567 B1
反应条件
hydrogenchloride in water 0.333333 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 23, # 12 p. 1356 - 1359
Khimiya Geterotsiklicheskikh Soedinenii, , # 12 p. 1683 - 1687
反应条件
1: 82 percent / SOCl2, conc. H2SO4 / 0.5 h / Heating 2: 67 percent / Fe / ethanol / 0.5 h / Heating 3: 97 percent / conc. hydrochloric acid / H2O / 0.33 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 23, # 12 p. 1356 - 1359
Khimiya Geterotsiklicheskikh Soedinenii, , # 12 p. 1683 - 1687
反应条件
ammonium hydroxide; sulfur dioxide T=120 - 130°C;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 3, p. 535 - 536
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 3, p. 666 - 667
反应条件
sulfuric acid; hydroxylamine
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 4, p. 587 - 588
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 4, # 5 p. 812 - 814
反应条件
1: S2Cl2 2: H2O 3: OH- / ethanol View Scheme
参考文献
Pesin,V.G.; Zolotova-Zolotukhina,L.V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 208 - 209
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, # 2 p. 314 - 315
反应条件
1: SO3/H2SO4
2: (i) NaNO2, aq. HCl, (ii) KClO3
View Scheme
参考文献
Pesin,V.G. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 4 p. 1267 - 1272,1265 - 1269