1,1'-[乙亚基二(氧基)]二丁烷合成路线 (共 77 条)
参考文献
Post
Journal of Organic Chemistry, 1940 , vol. 5, p. 247
反应条件
toluene-4-sulfonic acid; acetone-oxime in benzene
72 h; Ambient temperature; Further byproducts given. Title compound not separated from byproducts;
参考文献
Voronkov, M. G.; Keiko, N. A.; Shuvashev, Yu. A.; Kalikhman, I. D.; Keiko, V. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 49 - 52
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 57 - 60
反应条件
anhydrous heptafluorobutyric acid
T=95 - 100°C; 1.5 h; other reagent (trifluoroacetic acid); Further byproducts given;
参考文献
Trofimov, B.A.; Nedolya, N.A.; Komel'kova, V.I.; Voronkov, M.G.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1752
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1995 - 1996
反应条件
chloro-trimethyl-silane
参考文献
Lisovin, E. G.; Komarov, N. V.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 4 p. 854 - 859,688 - 692
反应条件
toluene-4-sulfonic acid in benzene
72 h; Ambient temperature; Further byproducts given. Title compound not separated from byproducts;
参考文献
Voronkov, M. G.; Keiko, N. A.; Shuvashev, Yu. A.; Kalikhman, I. D.; Keiko, V. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 49 - 52
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 1 p. 57 - 60
反应条件
1: HCl / 0 °C
View Scheme
参考文献
Schosstakowski; Bogdanowa
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 573
Chem.Abstr., 1948 , p. 4519
反应条件
toluene-4-sulfonic acid
参考文献
Beduwe
Bulletin des Societes Chimiques Belges, 1925 , vol. 34, p. 49
Chem. Zentralbl., 1925 , vol. 96, # I p. 1973
参考文献
Prileshajewa et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 560,565
Chem.Abstr., 1952 , # 7044
反应条件
acidic cationen-exchanger
参考文献
Mastagli et al.
Bulletin de la Societe Chimique de France, 1957 , p. 764
参考文献
Vlasov,V.M. et al.
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, # 12 p. 2137 - 2142,2095 - 2099