3-(甲基氨基)巴豆酸乙酯合成路线 （共 22 条）
反应条件
1: bei der Reduktion 2: alcoholic KOH-solution / Behandeln des Reaktionsgemisches mit Wasser View Scheme
参考文献
Knorr
Justus Liebigs Annalen der Chemie, 1886 , vol. 236, p. 296,298
Chemische Berichte, 1889 , vol. 22, p. 162
反应条件
in toluene 42 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7079 - 7083
反应条件
1: pyridine / diethyl ether / Ambient temperature 2: hydroxylamine hydrochloride, acetic acid / 0.5 h / Heating 3: 60 percent / pyridinium chlorochromate / CH2Cl2 / 72 h / Ambient temperature View Scheme
参考文献
Chantegrel, Bernard; Deshayes, Christian; Pujol, Bernard; Wei, Zhong Jia
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 927 - 934
参考文献
Barraja, Paola; Diana, Patrizia; Montalbano, Alessandra; Martorana, Annamaria; Carbone, Anna; Cirrincione, Girolamo
Tetrahedron Letters, 2009 , vol. 50, # 28 p. 4182 - 4184
参考文献
Grinew et al.
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 1355; engl. Ausg. S. 1301
参考文献
Knoevenagel
Chemische Berichte, 1903 , vol. 36, p. 2186
参考文献
Knorr
Justus Liebigs Annalen der Chemie, 1886 , vol. 236, p. 296,298
Chemische Berichte, 1889 , vol. 22, p. 162
参考文献
Yamato, Masatoshi; Sato, Koichi; Hashigaki, Kuniko; Ninomiya, Mayumi
Heterocycles, 1982 , vol. 19, # 7 p. 1263 - 1268
参考文献
Yamato, Masatoshi; Sato, Koichi; Hashigaki, Kuniko; Ninomiya, Mayumi
Heterocycles, 1982 , vol. 19, # 7 p. 1263 - 1268
反应条件
pyridine; hydroxylamine hydrochloride
1.) Et2O, RT, 48 h, 2.) AcOH, reflux, 0.5 h; Yield given. Multistep reaction;
参考文献
Chen, Ya Ping; Chantegrel, Bernard; Deshayes, Christian
Heterocycles, 1995 , vol. 41, # 1 p. 175 - 186
