7-乙氧基-4-甲基香豆素合成路线 (共 9 条)
反应条件
silica gel Pechmann condensation; 0.0333333 h; Microwave irradiation;
参考文献
Synthetic Communications, , vol. 40, # 22 p. 3358 - 3364
反应条件
1: 7-hydroxy-4-methyl-coumarin With potassium carbonate in acetone 0.5 h; 2: ethyl iodide With potassium iodide in acetone T=40°C; 120 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 77, p. 400 - 408
反应条件
boron trifluoride T=60°C; Pechmann reaction; 0.333333 h;
参考文献
Molecules, , vol. 10, # 3 p. 720 - 724
反应条件
1: ethyl acetoacetate; recorcinol With sulfuric acid T=10 - 25°C; 2: ethyl halide With potassium carbonate in N,N-dimethyl-formamide 6 h;
参考文献
Asian Journal of Chemistry, , vol. 25, # 12 p. 6609 - 6611
反应条件
oxygen; methylene blue in methanol 150 h; Irradiation;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 39, p. 199 - 204
反应条件
in tert-butyl alcohol Methylation; 15 h; UV-irradiation;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 38, # 6 p. 726 - 727
反应条件
ethanol; sodium ethanolate anschliessenden Erwaermen mit Aethylbromid;
反应条件
oxygen; methylene blue in methanol 150 h; Irradiationwith and without singlet oxygen; further solvent; Product distributionMechanism;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 39, p. 199 - 204
反应条件
(i) PtO2, EtOH, (ii) N2H4*H2O, benzene; Multistep reaction;
参考文献
Allen,C.F.H.; Weismann Magder,E.
Journal of Heterocyclic Chemistry, 1969 , vol. 6, p. 349 - 360