carbon tetrabromide; triphenylphosphine in dichloromethane
T=0 - 25°C; 3 h;
参考文献
Perchonock, Carl D.; Finkelstein, Joseph A.; Uzinskas, Irene; Gleason, John G.; Sarau, Henry M.; Cieslinski, Lenora B.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2457 - 2460
1: 92 percent / NaI / dimethylformamide / 3 h / 100 °C
2: 78 percent / Hydrogen / Pd, BaSO4, quinoline / ethyl acetate
3: 89 percent / KOH / methanol; H2O / 19 h / Heating
4: 72 percent / CBr4, PPh3 / CH2Cl2 / 3 h / 0 - 25 °C
View Scheme
参考文献
Perchonock, Carl D.; Finkelstein, Joseph A.; Uzinskas, Irene; Gleason, John G.; Sarau, Henry M.; Cieslinski, Lenora B.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2457 - 2460
Perchonock, Carl D.; Finkelstein, Joseph A.; Uzinskas, Irene; Gleason, John G.; Sarau, Henry M.; Cieslinski, Lenora B.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2457 - 2460
Perchonock, Carl D.; Finkelstein, Joseph A.; Uzinskas, Irene; Gleason, John G.; Sarau, Henry M.; Cieslinski, Lenora B.
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2457 - 2460
