in toluene byproducts: tBu2Sn(OH)Cl, LiI; dissoln. and cooling of I-compd. (-78°C), addn. of soln. of Ph3SnLi, stirring and removal of cooling (several h);
参考文献
Adams, Stefan; Draeger, Martin
Angewandte Chemie, 1987 , vol. 99, p. 1280 - 1282
in tetrahydrofuran byproducts: tBu2Sn(OH)Cl, LiI; dissoln. and cooling of I-compd. (-78°C), addn. of soln. of Ph3SnLi, stirring and removal of cooling (several h);
参考文献
Adams, Stefan; Draeger, Martin
Angewandte Chemie, 1987 , vol. 99, p. 1280 - 1282
