(R)-(+)-3-(乙酰硫基)异丁酸甲酯合成路线 (共 6 条)
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran 0 deg C, 1 h, RT.;
参考文献
Parry, Ronald J.; Mizusawa, A.E.; Chiu, I.C.; Naidu, M.V.; Ricciardone, M.
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2512 - 2521
反应条件
anhydrous sodium hydrogen carbonate in tetrahydrofuran
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5506267 A1, 1996 ;
反应条件
sodium hydroxide in phosphate buffer T=37°C; pH=6.8; 0.3 h;
参考文献
Organic Letters, , vol. 1, # 2 p. 207 - 209
反应条件
propan-1-ol in hexane T=25°C; 72 h; porcine pancreatic lipase; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 21 p. 5657 - 5659
参考文献
Bianchi, Daniele; Cesti, Pietro
Journal of Organic Chemistry, 1990 , vol. 55, # 21 p. 5657 - 5659
参考文献
US5266568 A1, ;
US 5266568 A