3-(4-甲基苯基)环戊酮合成路线 (共 5 条)
反应条件
sodium acetate; antimony trichloride; palladium diacetate in acetic acid
T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-ichi; Ohe, Kouichi; Uemura, Sakae; Shim, Sang Chul
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 883 - 888
反应条件
4,4'-bis(trimethylaminomethyl)-2,2'-bipyridine dihydrobromide; tetrafluoroboric acid; Pd(NH3)2Cl2 in water
T=80°C; pH=1; 24 h;
参考文献
Huang, Shao-Hsien; Wu, Tzu-Min; Tsai, Fu-Yu
Applied Organometallic Chemistry, 2010 , vol. 24, # 9 p. 619 - 624
反应条件
formic acid; phosphoric acid
T=80°C;
参考文献
Deb, Biswajit; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Journal of Chemical Research, Miniprint, 1990 , # 11 p. 2728 - 2758
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene
T=80°C; 2 h; Yields of byproduct given;
参考文献
Kamigata, Nobumasa; Satoh, Akira; Yoshida, Masato
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 46, p. 121 - 130
反应条件
bis(acetylacetonate)nickel(II); lithium; zinc dibromide
1.) ether, sonication, 45 min, 2.) ether, 0 deg C to room temp., 5 min; Yield given. Multistep reaction;
参考文献
Luche, Jean-Louis; Petrier, Christian; Lansard, Jean-Philippe; Greene, Andrew E.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3837 - 3839