二甲基2,5-二溴己二酸酯合成路线 （共 8 条）
反应条件
in methanol T=75°C; 56 h;
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 71 percent / methanol / 56 h / 75 °C 2: aq. HCl / 12 h / Heating View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 71 percent / methanol / 56 h / 75 °C 2: aq. HCl / 12 h / Heating 3: 180 °C / water pump View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
1: 71 percent / methanol / 56 h / 75 °C
2: aq. HCl / 12 h / Heating
3: 180 °C / water pump
4: 96 percent / SOCl2 / benzene / 24 h / 70 °C
View Scheme
参考文献
Daly, Adrian M.; Gilheany, Declan G.
Tetrahedron Asymmetry, 2003 , vol. 14, # 1 p. 127 - 137
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
McDonald,R.N.; Reitz,R.R.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2418 - 2423
反应条件
tetra-n-butylammonium perchlorate; sodium iodide in N,N-dimethyl-formamide
electrolysis: Pt cathode, Cu anode; Yield given. Yields of byproduct given;
参考文献
Tokuda, Masao; Hayashi, Atsushi; Suginome, Hiroshi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2590 - 2592
参考文献
Wille et al.
Justus Liebigs Annalen der Chemie, 1957 , vol. 608, p. 22,36
反应条件
Multi-step reaction with 2 steps 1: sodium azide / N,N-dimethyl-formamide2: hydrogenchloride; water; triphenylphosphine
参考文献
Cie, Dariusz; Kalinowska-Tucik, Justyna Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-Z0069-OP, p. 1736 - 1744
