1-叠氮基-3,6,9-三氧杂十一烷-11-醇合成路线 （共 26 条）
反应条件
sodium azide in acetonitrile 18 h; Heating;
参考文献
Cubberley; Iverson
Journal of the American Chemical Society, 2001 , vol. 123, # 31 p. 7560 - 7563
反应条件
sodium azide in ethanol Reflux;
参考文献
Leal, Manuel Pernia; Assali, Mohyeddin; Fernandez, Inmaculada; Khiar, Noureddine
Chemistry - A European Journal, 2011 , vol. 17, # 6 p. 1828 - 1836
反应条件
sodium hydroxide in tetrahydrofuran; ethanol; water; ethyl acetate
参考文献
Sanofi-Aventis
Patent: EP1574516 A1, 2005 ;
反应条件
in methanol; chloroform
参考文献
The State of Oregon Acting by and through the State Board of Higher Education on behalf of the University of Oregon
Patent: US5135737 A1, 1992 ;
反应条件
1: 85 percent / triethylamine / CH2Cl2 / 20 h / 20 °C 2: 76 percent / sodium azide / ethanol / 7 h / 85 °C View Scheme
参考文献
Pharmaceutical Research, , vol. 22, # 8 p. 1411 - 1421
反应条件
sodium azide; dimethyl sulfoxide T=60°C; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 119, # 35 p. 8363 - 8364
反应条件
sodium azide; sodium chloride in ethanol; dichloromethane; ethyl acetate; toluene
参考文献
Saxon, Eliana; Bertozzi, Carolyn Ruth
Patent: US2002/16003 A1, 2002 ;
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 2 h;
参考文献
Bertozzi, Carolyn R.; Bednarski, Mark D.
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4326 - 4329
反应条件
toluene-4-sulfonic acid in methanol
参考文献
Bondia, Andrea Molero; Larcher, Nicolas; Garrelly, Laurent; Rossi, Jean Christophe; Pascal, Robert
Tetrahedron Letters, 2010 , vol. 51, # 25 p. 3330 - 3333
反应条件
1: With pyridine; p-toluenesulfonyl chloride in tetrahydrofuran T=20°C; 2.5 h; Inert atmosphere; 2: With sodium azide in ethanol 12 h; Reflux;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 9 p. 2151 - 2154
