S-甲基异硫脲半硫酸盐合成路线 (共 119 条)
反应条件
in ethanol Heating10-12 h; Yield given;
参考文献
Agarwal, Anu; Srivastava, Kumkum; Puri; Chauhan, Prem M.S.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 12 p. 3133 - 3136
参考文献
Pant,E.
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1964 , vol. 335, p. 272 - 274
反应条件
sodium methylate in methanol; dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
Yamanaka, Hiroki; Takekawa, Tadashi; Morita, Kenji; Ishihara, Takashi; Gupton, John T.
Tetrahedron Letters, 1996 , vol. 37, # 11 p. 1829 - 1832
反应条件
1: in water 2 h; Reflux; 2: With BaCl2 in water 1.5 h; Reflux;
参考文献
Guo, Dexiang; Liu, Yajing; Li, Ting; Wang, Nan; Zhai, Xin; Hu, Chun; Gong, Ping
Science China Chemistry, 2012 , vol. 55, # 3 p. 347 - 351
反应条件
1: 2-methyl-2-thiopseudourea sulfate; methyl chloroformate With sodium hydroxide T=10 - 15°C; pH=8.0; 2: 4-Chloro-benzene-1,2-diamine With acetic acid T=95°C; pH=5.0; 2 h;
参考文献
Valdez, Juan; Cedillo, Roberto; Hernandez-Campos, Alicia; Yepez, Lilian; Hernandez-Luis, Francisco; Navarrete-Vazquez, Gabriel; Tapia, Amparo; Cortes, Rafael; Hernandez, Manuel; Castillo, Rafael
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 16 p. 2221 - 2224
反应条件
sodium in ethanol 1 h; Heating;
参考文献
Palanki, Moorthy S.S.; Erdman, Paul E.; Goldman, Mark E.; Suto, Carla; Suto, Mark J.
Medicinal Chemistry Research, 2000 , vol. 10, # 1 p. 19 - 29
反应条件
sulfuric acid; nitric acid
参考文献
Northwestern University
Patent: US7470815 B1, 2008 ;
Location in patent: Page/Page column 37 ;
反应条件
in water 0.25 h; Heating;
参考文献
Agarwal, Anu; Srivastava, Kumkum; Puri; Chauhan, Prem M.S.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 12 p. 3133 - 3136
反应条件
sodium acetate in N,N-dimethyl-formamide T=20 - 80°C; 2 h;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 23 p. 10652 - 10661
反应条件
sodium hydroxide Heating;
参考文献
Effenberger, Franz; Beisswenger, Thomas; Dannenhauer, Fritz
Chemische Berichte, 1988 , vol. 121, p. 2209 - 2224