4-甲氧基-2,3,5-三甲基吡啶-n-氧化物合成路线 （共 23 条）
反应条件
hydrogenchloride; titanium(III) chloride in water 2 h;
参考文献
Pharmazie, , vol. 52, # 9 p. 686 - 691
反应条件
1: 110 °C 2: aq. NaOH / methanol / Heating 3: 90 percent / SOCl2 / CH2Cl2 / 0.5 h / Heating View Scheme
参考文献
Sharada; Satyanarayana Reddy; Sammaiah; Sumalatha
Asian Journal of Chemistry, 2013 , vol. 25, # 14 p. 7959 - 7966
反应条件
1: 110 °C 2: aq. NaOH / methanol / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 11 p. 1777 - 1788
反应条件
1: With p-toluenesulfonyl chloride in dichloromethane T=40°C; 2 h; 2: With triethylamine in dichloromethane T=40°C; 3 h;
参考文献
Weidmann, Klaus; Herling, Andreas W.; Lang, Hans-Jochen; Scheunemann, Karl-Heinz; Rippel, Robert; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 3 p. 438 - 450
反应条件
1.1: pTsCl / CH2Cl2 / 2 h / 40 °C 1.2: Et3N / CH2Cl2 / 3 h / 40 °C 2.1: 2.1 g / methanol / 4 h / Heating View Scheme
参考文献
Rane; Pathak; Kaushik; Prasad Rao; Kumar, Ashok
Synthetic Communications, 2002 , vol. 32, # 8 p. 1211 - 1217
参考文献
Aktiebolaget Hassle
Patent: US4785113 A1, 1988 ;
反应条件
sodium methylate in methanol
参考文献
Otsuka Pharmaceutical Co., Ltd.
Patent: US5670526 A1, 1997 ;
反应条件
palladium monocarbide in water; acetic acid; toluene
参考文献
Aktiebolaget Hassle
Patent: US4785113 A1, 1988 ;
反应条件
sodium hydroxide; nitric acid in methanol; conc. H2 SO4; toluene
参考文献
Aktiebolaget Hassle
Patent: US4544750 A1, 1985 ;
反应条件
dihydrogen peroxide in acetic acid
30 deg C, 1 h -> 70 deg C, 5 h -> 90 deg C;
参考文献
Mittelbach, Martin; Schmidt, Hans-Werner; Uray, Georg; Junek, Hans; Lamm, Bo; et al.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 8 p. 524 - 529
